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preconcentration of molybdenum from a low

  • The Determination of Molybdenum in Seawater by ICP-AES ...

    2.4.2.11 Preconcentration Facto33 r and Detection Limit 2.4.2.12 Determination of Mo(VI3) in Seawate3 r by ICP-AES ... Low dietary molybdenum leads to low urinary and serum uric acid concentrations and . o excessive xanthine excretion. As a constituent of the nitrate reductase and nitrogenase of plants, molybdenum


  • Determination of a Trace Amount of Molybdenum(VI) by ...

    in 1992 molybdenum was also regulated as a monitor-ing item in tap water, and the tolerable concentration was under 0.07 mg dm-3. It is difficult, however, to directly determine molybdenum in environmental sam-ple solutions, because it exists at a low concentration level; thus, preconcentration methods, such as solvent


  • New chelating resin for preconcentration and determination ...

    preconcentration–separation procedures have been proposed. Preconcentration is a very important issue for achievement of low detection limits (Prabhakaran and Subramanian, 2003). There are many methods of preconcentration and separation such as liquid–liquid extraction ( Saito et al., 2000 ) ion exchange techniques (Alguacil et al., 2005),


  • Preconcentration of molybdenum, antimony and vanadium in ...

    Jun 15, 2013· Highlights Dowex 1-x8 SPE method for preconcentration of trace metals in gasoline is reported. The method had relatively high enrichment factor with low LOD and LOQ values. The column can be reused up to 150 cycles without significant loss of sorption performance. The method was applied for analysis of real gasoline samples.


  • Determination of low levels of molybdenum (VI) in food ...

    Nov 01, 2013· Read "Determination of low levels of molybdenum (VI) in food samples and beverages by cloud point extraction coupled with flame atomic absorption spectrometry, Journal of Food Composition and Analysis" on DeepDyve, the largest online rental service for scholarly research with thousands of academic publications available at your fingertips.


  • Journal of Chemistry - Hindawi Publishing Corporation

    An extractive spectrophotometric method has been developed for microdetermination of molybdenum. At room temperature Mo(VI) was reduced to Mo(V) in 2 M H2SO4 using ascorbic acid as a reductant. The Mo(V) formed a yellow-coloured (1 : 2) complex with 6-chloro-3-hydroxy-2-(3 -hydroxyphenyl)-4-oxo-4H-1-benzopyran (CHHB). The complex was quantitatively extracted into toluene and absorbed maximum ...


  • Liquid chromatography–electrothermal atomic absorption ...

    To permit the molybdenum preconcentration as described in the next section, a procedure was developed to transform Mo associated to proteins in inorganic Mo (molybdate), based on the thermal treatment of milk with 0.02% tetramethylammonium hydroxide (TMAH).


  • Studies on the Solid Phase Extraction and Preconcentration ...

    Studies on the Solid Phase Extraction and Preconcentration of Zirconium, Hafnium, Molybdenum, and Tungsten With Chitin for Their Determination in Geological Samples …


  • Solid-Phase Extraction and Spectrophotometric ...

    A method for the preconcentration and determination of molybdenum(VI) in soil and plant samples using Amberlite XAD-7 resin and spectrophotometry is proposed. ... are difficult because of its low ...


  • Measurement of the Isotopic Composition of Molybdenum in ...

    Measurement of the Isotopic Composition of Molybdenum ... A novel preconcentration method is presented for the ... and low total proce-dural blank (~ 0.18 ng).


  • Preconcentration of molybdenum, antimony and vanadium in ...

    Preconcentration of molybdenum, antimony and vanadium in gasolsine samples using Dowex 1-x8 resin and their determination with inductively coupled plasma-optical emission spectrometry


  • Application of 1,2-Dihydroxybenzene-3,5-disulfonic Acid ...

    Alternatively, molybdenum can be quantitatively adsorbed on Tiron-TDBA-naphthalene adsorbent packed in a column and determined in a similar manner. About 0.02 µg of molybdenum can be concentrated in a column from 500 mL of aqueous sample, where its concentration is as low …


  • Determination of molybdenum in sea and estuarine water ...

    Abstract. An analytical method has been developed for the determination of submicrogram quantities of molybdenum in sea and esturaine water. The method consists of preconcentration of molybdenum with BETA-naphthoin oxime followed by the determination of the …


  • Utilization of Cloud-Point Preconcentration for ...

    determination of molybdenum [3–22]. Owing to their low sensitivity and selectivity, preconcentration and/or separation steps are usually necessary. There have been reported highly sensitive analytical techniques for the molybdenum determination such as spectrofluorimetry [23], voltammetry [24,25],


  • Preconcentration of Molybdenum from a Low-grade Primary Mo ...

    Studies on pre-concentration of molybdenum values from a primary molybdenum ore deposit located in Harur of Dharmapuri district, Tamilnadu were carried out by physical beneficiation techniques. Inspite of being a primary deposit, the Mo content in the ore is very low, being 0.06% only. Mo is present as molybdenite (MoS 2 ) and the other sulfide minerals in the ore are pyrite, galena and traces ...


  • PRECONCENTRATION OF TRACE III. PRECONCENTRATION …

    PRECONCENTRATION OF TRACE ... Traces of ions, generally complex ions, at the low ppm level or less in an aqueous solution are floated with the aid of surfactant ions of opposite charge to the ions. ... Example 2: Preconcentration of traces of molybdenum(VI) in seawater (Ref. 6).


  • The use of long-chain alkylamines for preconcentration of ...

    Long-chain alkylamines are used for the preconcentration of traces of molybdenum, tungsten and rhenium as thiocyanate complexes, in their determination by atomic-absorption spectroscopy. General studies of factors, influencing the extraction show that the thiocyanate complexes can be extracted into chloroform containing a low concentration of ...


  • Pre-Concentration and Determination of Molybdenum in …

    of 25% and 58% have been reported at molybdenum concentrations of 1.2 μg L-1and 0.6 μg L-1, respectively (Johannesson, Lyons, Graham, & Welch, 2000; Jones & McLain, 1997). Therefore, pre-concentration is essential when analyzing natural water samples for molybdenum at very low concentrations. The use of chelating resins to


  • molybdenum ore grind for flotation

    Preconcentration of Molybdenum from a Low-grade, Studies on pre -concentration of molybdenum values from a primary molybdenum ore deposit located in Harur, 311Mesh -of grind Figure 2 Flotation response of Harur molybdenite ore as a function of, Preconcentration of Molybdenum from a Low-grade Primary Mo Ore by Physical Beneficition 98


  • Determination of low levels of molybdenum (VI) in food ...

    Selective CPE method proposed for determination of low levels of molybdenum. • Detection limit, 2.18 μg L −1, 100-fold preconcentration factor in wide linear range.. The feasibility of Mo analysis in beverages, foods was demonstrated based on CPE.


  • Molybdenum Deficiency Symptoms | Livestrong.com

    Molybdenum is an essential trace element that contributes to the functions of your nervous system and kidneys. Molybdenum also plays a role in energy production on a cellular level. Although the specific functions of molybdenum are not well understood, the American Cancer Society notes that this ...


  • Pyrocatechol Violet in New Optical Methods for Determining ...

    The complexation of molybdenum(VI) with Pyrocatechol Violet (PCV) in the absence or presence of a cationic surfactant, cetyltrimethylammonium (CTMA), was studied. Conditions for the preconcentration of molybdenum(VI) as its PCV complex on adsorbents of different nature were found.


  • Determination of low levels of molybdenum (VI) in food ...

    Determination of low levels of molybdenum (VI) in food samples and beverages by cloud point extraction coupled with flame atomic absorption spectrometry


  • New chelating resin for preconcentration and determination ...

    US Environmental Protection Agency How to cite this article A New chelating resin for preconcentration and determination of molybdenum by inductive couple plasma atomic emission spectroscopy Jan ...


  • Determination of Molybdenum in Environmental Samples ...

    Determination of molybdenum in different kinds of environmental samples is often a challenging task for analysts. Its concentration is usually very low and the sample matrix may cause serious ...